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Self sensitized photooxidation of tetrathienyltetrathiafulvalenes: synthesis of thienyl substituted 1,2,5,8-tetrathiecine-6,7-dione, a new heterocyclic system

Charlton, A. and Donati, D. and Fusi, S. and Murphy, P.J. and Ponticelli, F. (2013) Self sensitized photooxidation of tetrathienyltetrathiafulvalenes: synthesis of thienyl substituted 1,2,5,8-tetrathiecine-6,7-dione, a new heterocyclic system. Tetrahedron Letters, 54 ((10)). pp. 1227-1229. DOI: 10.1016/j.tetlet.2012.12.080

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Abstract

Irradiation of tetrathienyltetrathiafulvalenes in an oxygen saturated solution gives tetrathienyl substituted 1,2,5,8-tetrathiecine-6,7-diones, via singlet oxygen generation followed by cycloaddition onto the TTF double bond and a final rearrangement process. The thermal and photochemical behaviour and reductive methylation of this new class of macro-heterocyclic system have also been investigated.

Item Type: Article
Subjects: Research Publications
Date Deposited: 09 Dec 2014 16:44
Last Modified: 23 Sep 2015 03:07
ISSN: 0040-4039
URI: http://e.bangor.ac.uk/id/eprint/937
Identification Number: DOI: 10.1016/j.tetlet.2012.12.080
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